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18.1 Products List
Outre is a technological enterprise which is specialized in research, production of pipelines and steel bar anticorrosion coating, and it is a new company which is in the integrated mode of researching, producting and saling. Our staff have committed to the research and development of the anticorrosion industry over the years. Following the principles of serialization, diversification and specialization, we have invented the following products successfully:
|
Product Name |
Type |
Application Scope |
|
3PE anticorrosion powder coating |
SP-13 |
suitable for the ordinary 3PE external anticorrosion coating |
|
SP-13A1 |
suitable for the pipelines with large diameter in long transmission，60℃ cathodic disbonding resistant for 30d of 3PE external anticorrosion coating |
|
|
SP-13A |
suitable for GB/T23257-2009 and those that are equal to the domestic and international technical standards of 3PE external anticorrosion coating |
|
|
SP-13B |
suitable for the coating temperature between 190°C -200C°, performance indicators of curing coating reached GB/T23257-2009 and those that are equal to the domestic and international technical standards of 3PE external anticorrosion coating |
|
|
dual—layer fusion bonded epoxy powder coating |
SP-12 |
suitable for anticorrosion coating of traversing and elbow pipelines |
|
single—layer fusion bonded epoxy powder coating |
SP-11 |
suitable for FBR structure external anticorrosion coating |
|
internal epoxy powder coating |
SP-21 |
suitable for water delivery, high temperature media and wear resistance pipelines of internal anticorrosion coating |
|
steel bar anticorrosion coating |
SB-11 |
suitable for steel bar architectural of anticorrosion coating |
|
bituminous epoxy anticorrosion paint |
OT—0 01A/OT—001B |
applied to containers, ships, port facilities, offshore drilling platforms, underground gas pipelines, water pipelines, oil pipelines, gas containers and so on |
|
epoxy leakproof agent |
SP-31 |
fusion bonded epoxy powder coating of supplement ingredients and protection of joint coating, elbows, shaped tubes quick-drying and easy construction |
|
inner resistance- reducing coating |
OT-003(A、B components) |
suitable for large diameter natural gas pipelines |
|
thick paste epoxy-phenolics coating for inner surface |
OT-005 |
suitable for storage tanks and pipelines of inner surfaces |
|
epoxy zinc-rich primer |
OT-008 |
applied to long-term anticorrosion of containers, ships, port facilities, offshore oil production equipments, chemical equipments and steel structure, etc |
|
epoxy primer/ topcoat |
OT-010 |
for the anticorrosion of different materials such as iron, zinc, aluminum and stainless steel |
|
epoxy micaceous iron oxide intermediate paint |
OT-012 |
used for bridges, ships and marine facilities, etc in the atrocious environment |
18.2 The Main Technical Indicators of Products
18.2.1 The Technical Indicators of SP-13A Which Is Used as a Underlying Epoxy External Anticorrosion Powder Coating at Room Temperature
For the requirement of the epoxy powder which is used for the 2nd Chinese West-East Pipeline Project and based on the SP-13A1（60℃ cathodic disbonding resistant for 30d） which is used for Sichuan-East Gas Pipeline Project, we have invented SP-13A epoxy powder. It is suitable for 65℃ cathodic disbonding resistance for 30d and -30℃ low-temperature bending, according to the national standard GB/T23257-2009.
1）Powder Properties
|
Test Project |
Technical Specification |
Test Method |
|||
|
appearance |
uniform color and no agglomerations |
visual inspection |
|||
|
density |
1.30-1.50 |
GB/T 4472-1984 |
|||
|
content of volatile |
≤0.6% |
GB/T 6554 |
|||
|
size distribution |
150μm sieve powder 250μm sieve powder |
≤3.0% ≤0.2% |
GB/T 6554-1986 |
||
|
gelling time(s) |
200℃ |
≥12 |
GB/T 6554 |
||
|
curing time(min) |
200℃ |
≤3 |
GB/T23257-2009 appendix A |
||
|
thermal characteristic |
reaction heat △H J/g |
≥45 |
GB/T23257-2009 appendix B |
||
|
glass transition temperature Tg 2℃ |
≥95 |
GB/T23257-2009 appendix B |
|||
2）Coating Performances
|
Project |
Unit |
Technical Specification |
Experimental Method |
|
adhesion strength |
level |
≤2 |
GB/T23257-2009 appendix G |
|
cathodic disbonding resistance (65℃ 48h) |
mm |
≤8 |
GB/T23257-2009 appendix D |
|
cathodic disbonding resistance (65℃ 30d) |
mm |
≤15 |
GB/T23257-2009 appendix D |
|
bending resistant（-30℃ 2.5°） |
/ |
no cracks |
GB/T23257-2009 appendix E |
18.2.2 The Technical Indicators of SP-13B Which Is Used as a Underlying External Anticorrosion Epoxy Powder Coating at Low Temperature
For the requirement of epoxy powder which is used for the 2nd Chinese West-East Pipeline Project, we have invented SP-13B epoxy powder. It is suitable for 65℃ cathodic disbonding resistant for 30d and -30℃low-temperature bending, according to the national standard GB/T23257-2009.
1）Powder Properties
|
Test Project |
Technical Specification |
Test Method |
||
|
appearance |
uniform color and no agglomerations |
visual inspection |
||
|
density |
1.30-1.50 |
GB/T 4472-1984 |
||
|
content of volatile |
≤0.6% |
GB/T 6554 |
||
|
size distribution |
150μm sieve powder 250μm sieve powder |
≤3.0% ≤0.2% |
GB/T 6554-1986 |
|
|
gelling time（s） |
200℃ |
≥12 |
GB/T 6554 |
|
|
curing time(min) |
190℃ |
≤3 |
GB/T23257-2009 Appendix A |
|
|
thermal characteristic |
reaction heat △H J/g |
≥45 |
GB/T23257-2009 appendix B |
|
|
glass transition temperature Tg 2℃ |
≥95 |
|||
2）Coating Performances
|
Project |
Unit |
Technical Specification |
Experimental Method |
|
adhesion strength |
level |
≤2 |
GB/T23257-2009 appendix G |
|
cathodic disbonding resistance (65℃ 48h) |
mm |
≤8 |
GB/T23257-2009 appendix D |
|
cathodic disbonding resistance (65℃ 30d) |
mm |
≤20 |
GB/T23257-2009 appendix D |
|
bending resistance（-30℃ 2.5） |
/ |
no crack |
GB/T23257-2009 appendix E |
18.2.3 The Technical Indicators of SP-13 Which Is Used as a Underlying External Anticorrosion Epoxy Powder Coating at Room Temperature
According to the requirement of the standard SY/T0413-2002, our product of 3PE ordinary anticorrosion epoxy powder is widely used in gas distribution network home and abroad.
1）Powder Properties
|
Test Project |
Technical Specification |
Test Method |
||
|
content of volatile |
≤0.6% |
GB/T 6554 |
||
|
size distribution |
150μm sieve powder 250μm sieve powder |
≤3.0% ≤0.2% |
GB/T 6554-1986 |
|
|
gelling time（s） |
200℃ |
≥12 |
GB/T 6554 |
|
|
curing time(min) |
200℃ |
≤3 |
SY/T0315-2005 Appendix A |
|
2）、Coating Performances
|
Projects |
Units |
Technical Specifications |
Experimental Methods |
|
adhesion strength |
level |
≤2 |
SY/T 0315-2005 appendix G |
|
cathodic disbonding resistance (65℃ 48h) |
mm |
≤8 |
GB/T23257-2009 appendix A |
18.2.4 The Technical Indicators of FBE Single-Layer Anticorrosion Powder Coating
1) Powder Properties
|
Test Project |
Technical Specification |
Test Method |
||
|
appearance |
uniform color and no agglomerations |
visual inspection |
||
|
density |
1.30-1.50 |
GB/T 4472 |
||
|
content of volatile (%) |
≤0.6 |
GB/T 6554 |
||
|
magnetics content （%） |
≤0.002 |
JB/T 6570 |
||
|
size distribution |
150μm sieve powder 250μm sieve powder |
≤3.0% ≤0.2% |
GB/T 6554 |
|
|
gelling time（s） |
230℃ |
≤30 |
GB/T 6554 |
|
|
180℃ |
≤90 |
|||
|
curing time(min) |
230℃ |
≤1.5 |
SY/T0315-2005 |
|
|
180℃ |
≤5.0 |
|||
|
thermal characteristic |
given characteristics comply with the powder manufacturers |
SY/T0315-2005 |
||
2）Coating Performances
|
Project |
Unit |
Technical Specification |
Experimental Method |
|
appearance |
/ |
smooth, uniform color , no bubbles , no cracks and shrinkage |
visual inspection |
|
adhesion strength |
level |
≤3 |
SY/T 0315-2005 appendix G |
|
1.5J shock resistance (-30℃) |
/ |
no leakage points |
SY/T 0315-2005 |
|
3°bending resistance |
/ |
no cracks |
SY/T 0315-2005 |
|
cathodic disbonding resistance (48h or 24h) |
mm |
≤6.5 |
SY/T 0315-2005 |
|
cathodic disbonding resistance (28d) |
mm |
≤8.5 |
SY/T 0315-2005 |
|
anti-chemical corrosion |
/ |
qualified |
SY/T 0315-2005 |
|
fracture porosity |
level |
1-3 |
SY/T 0315-2005 |
|
porosity of binding surface |
level |
1-3 |
SY/T 0315-2005 |
|
electric strength |
≥30 |
GB/T1408 |
|
|
volume resistivity |
≥1×1013 |
GB/T1410 |
|
|
wear rate（falling abrasive） |
/ |
≥3 |
SY/T 0315-2005 |
18.2.5 The Technical Indicators of SP-12 Which Is Used as a Double External Anticorrosion Epoxy Powder Coating
1）、Powder Properties
|
Test Project |
Technical Specification |
Test Method |
|
|
appearance |
uniform color and no agglomerations |
visual inspection |
|
|
density g/cm3 |
inner layer |
1.3-1.5 |
GB/T4472 |
|
outer layer |
1.5-1.8 |
||
|
content of volatile |
inner layer |
≤0.6 |
Q/CNPC 38-2002 appendix B |
|
outer layer |
≤0.6 |
||
|
size distribution |
150μm sieve powder ≤4.0% 250μm sieve powder ≤0.2% |
Q/CNPC 38-2002 appendix C |
|
|
gelling time（s） 230℃ |
inner layer |
≥12 |
Q/CNPC 38-2002 appendix A |
|
outer layer |
≥12 |
||
|
curing time(min) 205℃ |
inner layer |
≤3 |
SY/T 0315-2005 appendix A |
|
outer layer |
≤3 |
||
|
magnetics content |
inner layer |
≤0.002 |
GB/T 2482-1986 |
|
outer layer |
≤0.002 |
||
|
thermal characteristic |
given characteristics comply with the powder manufacturers |
SY/T 0315-2005 appendix B |
|
2）、Coating Performances
|
Project |
Technical Specification |
Experimental Method |
|
|
appearance |
smooth, uniform color , no bubbles , no cracks and shrinkage |
visual inspection |
|
|
adhesion strength (level) |
1-2 |
SY/T0315-2005 appendix G |
|
|
shock resistance 10J |
no pinholes |
Q/CNPC 38-2002 appendix E |
|
|
2° bending resistant (-30℃±3℃) |
no cracks |
Q/CNPC 38-2002 appendix D |
|
|
cathodic disbonding （1.5V，65℃±3℃48h） |
≤6mm |
SY/T0315-2005 appendix C |
|
|
cathodic disbonding （1.5V，20℃±3℃28d） |
≤8mm |
SY/T0315-2005 appendix C |
|
|
anti-chemical corrosion |
qualified |
SY/T0315-2005 |
|
|
fracture porosity（level） |
inner layer |
1-4 |
SY/T0315-2005 appendix D |
|
porosity of binding surfaces(level) |
outer layer |
1-4 |
SY/T0315-2005 appendix D |
|
electric strength |
≥30 |
GB/T1408-1989 |
|
|
volume resistivity |
≥1×10¹³ |
GB/T1410-1989 |
|
|
wear rate（falling abrasive） |
≥3.5 |
SY/T0315-2005 |
|
|
30kg scratch resistance |
the remaining thickness of the coating is not less than the minimum design thickness of the inner |
Q/CNPC 38-2002 appendix F |
|
18.2.6 The Technical Indicators of SP-21 Which Is Used as an Internal Anticorrosion Epoxy Powder Coating
1）、Powder Properties
|
Test Project |
Technical Specification |
Test Method |
|
appearance |
uniform color and no agglomerations |
visual inspection |
|
density |
1.3-1.5 |
GB/T4472-1984 |
|
size distributions（%） |
150μm sieve powder 3.0% 250μm sieve powder 0.2% |
GB/T6554-1986 |
|
content of volatile（%） |
≥99.4 |
GB/T6554-1986 |
|
gelling time 200℃（s） |
≤120 |
GB/T6554-1986 |
|
level of liquidity（mm） |
22～28 |
GB/T6554-1986 |
|
magnetic content（%） |
≤0.002 |
GB/T2482-1986 |
2）、Coating Performances
|
Project |
Technical Specification |
Experimental Method |
|
|
appearance |
surface smooth, uniform color, no bubbles, no cracks, no shrinkages, and mild orange peel patterns are allowed |
visual inspection |
|
|
impact strength（J） |
≥11 |
Q/SJ0084-2003 appendix A |
|
|
wear resistance （1000g，1000r） |
≤20 |
GB/T1768-1979 |
|
|
adhesion strength (level) |
1-3 |
Q/SJ0084-2003 appendix B |
|
|
4° bending resistant |
the coating has no crack-free |
Q/SJ0084-2003 appendix C |
|
|
volume resistivity(Ω·m) |
≥1×1013 |
GB/T1410-1989 |
|
|
electric strength(MV/m) |
≥30 |
GB/T1408-1989 |
|
|
cathodic disbonding （65℃，48h） |
≤8 |
SY/T0413-95 |
|
|
salt spray test(1000h) |
The coating does not change |
GB/T1771-1991 |
|
|
resistance to chemical corrosion medium |
qualified |
10% HCl，at room temperature，90d 10% H2SO4，at room temperature,90d 3.5% NaCl，at room temperature,90d 10% NaOH，at room temperature,90d |
GB/T1763-1979 |
|
qualified |
oilfield wastewater，80℃，90d crude oil，80℃，90d gasoline，at room temperature，90d diesel，at room temperature，90d kerosene，at room temperature，90d |
GB/T1733-1993 |
|
18.3 The Performance Description of Outre Productions
18.3.1 Good Level Liquidity
To ensure the high stability, uniformity and good atomization of sprayed powder, and that epoxy powder could be uniformly coated on the surface of the steel pipes, Outre purchased professional testing equipment, fluidized instrument, and the level liquidity indicators are controlled in production process, to ensure that the epoxy powder evenly coated in onsite construction.
18.3.2 Good Powder Utilization
Size distribution：Most of ultrafine powder and coarse powder in the products have been removed after our technical improving and reformation. Thus our products have excellent size distribution and greatly improving the powder utilization.
18.3.3 Good storage stability
By using the resins which have high glass transition temperature and adding Tiyanium p25 to the products, the heat resistance of epoxy powder storage stability is greatly improved.
18.3.4 Good Coating Stability
Outre has set up the "products similarity" testing indicator in the finished products detection. We carry out the "products similarity" tests for each reactor to make sure that the similarity between each reactor of products is 99.5% at least. Thus ensuring the coating operation has a good stability. The products similarity detection records are as follows：
18.3.5 Good Construction Performance
We add the special additives in the production process, and we bought “Dry Powder Flow Meter”. Fluidization state in the production of finished products is controlled strictly, to ensure good powder liquidity. This guaranteed fine spraying uniformity in onsite constructions. In addition, reaction promoters are added in the production process, which greatly improves the reaction activity and reduces the usage temperature of the products, so as to expand the temperature range of the products greatly.
19.1.2 Raw materials testing methods
A. Similarity testing of raw materials
1. Determination significance of the similarity of raw materials: the quality and stability of the powder product depends entirely on the similarity of the raw materials if the formulation and production process is completely fixed.
2．Experiment instruments：FTIR Infrared Spectrometer
3. Experimental principle
When samples was irradiated by infrared light with continuous change frequency, the molecules absorb certain frequency radiation, and the vibration or rotation causes the net change of dipole moment, resulting the molecular vibrational and rotational level from the ground state to the excited state transition, so that the transmitted light intensity corresponding to the absorption region was weaken. The infrared spectrum curve could be got once the percentage of infrared light transmittance and wavelength is recorded, and it can be qualitative, quantitative and structural analysed.
Infrared quantitative analysis not only can be used for quantitative analysis of single component but also can carry quantitative analysis on multi-component samples. It is needn’t to separate infrared quantitative analysis, and FTIR analysis is not limited by the sample state. Gas, solid and liquid all can be analyzed.
Outre's raw materials and filler are analysed by infrared when the raw materials come into factory and compare with each batch. According to the scanned figure, we can characterize the similarities of raw materials and the fillers, so to ensure the high quality stability of final products.
B. Determination of the glass transition temperature (Tg0) of the resin and curing agent
1. Determination of significance of Tg0
The glass transition temperature (Tg0) of the resin and curing agent directly affect the glass transition temperature of powder products(Tg1)，and then determines the storage stability of the powder product, so it is very important to determine and control Tg0.
2. Experiment instruments：DSC Differential Scanning Calorimetry
3. Experimental principle
Its basic principle is to use the external heating mode that makes the block heated evenly. Transfer heat to sample pan and reference pan through two ways, namely, air and thermal gasket made by constantan. The temperature of sample pan is detected by high sensitivity thermocouple composed of nichrome wire and nickel aluminum wire, and the temperature of reference pan is detected by thermocouple composed of nichrome wire and Constantan.
三、other detection indicators
In addition to the above indicators, Outre controls other indicators of the raw materials strictly, such as hydrochloric acid- acetone solution determination of epoxy value, global determination softening point, and organic chlorine, inorganic chlorine, volatile, magnetic material, colour and lustre, sieve residue, acetone dissolve slide, melting range, etc.
For a detailed understanding of these indicators measuring methods, please call to ask for details.
19.3 A list of testing equipment
|
Number |
Devicename |
Specification |
Manufacturer |
Functional Description |
Commissioning Date |
|
01 |
FTIR infrared spectrometer |
SpectrumBX |
USA PerkinElmer |
Inorganic and organic structure identification |
08.7 |
|
02 |
DSC differential scanning calorimetry |
6220 |
JAN |
To characterize thermal characteristics of the various raw materials and finished goods, such as curing percentage of powder coating and glass transition temperature difference |
07.6 |
|
03 |
Atomic absorption spectrometry |
AAanalyst 300 |
USA |
To analyze the content of metal elements in a variety of raw materials , to provide information on harmful metal impurity content of the organic raw materials , and also to determine the purity of the pigments and fillers |
06.6 |
|
04 |
Infrared thermometer |
LS-POP |
Germany Optris |
To monitor and record the temperature of the steel , to provide temperature control data |
08.4 |
|
05 |
Thickness gauge |
QuaNix 1500 |
Germany |
To measure film thickness, reaching the eligibility of the tested sample |
06.9 |
|
06 |
Laser particle size analyzer |
LS-POP（V）AIX-C1002 |
Zhuhai Europe and the United States grams technology co., LTD. |
To uniformly disperse sample, accurately measure the particle size distribution of the powder coating to ensure that the charge amount of the powder and the powder utilization |
05.8 |
|
07 |
Electronic precision balance |
FA2004 |
Tianjin TianMa instrument Co. , Ltd. |
To precisely measure the quality of raw materials and finished products , thereby calculate the density accurately |
08.1 |
|
08 |
Abrasive magnetic material analyzer |
JSII-G1 |
Zhengzhou Institute of abrasives grinding |
To measure the magnetic material content of a variety of raw materials and finished products |
05.4 |
|
09 |
Mechanical overweight analytical balance |
TG-328B |
Balance Instrument Co. , Ltd. in Tianjin |
To accurately weight for DSC experiments |
03.6 |
|
10 |
High impedance meter |
ZC36 |
Shanghai Precision Instrument Co., Ltd. |
To measure the surface resistivity and volume resistivity |
06.5 |
|
11 |
Steel bending instrument |
GW40 |
HeNan Morrowind Machinery Factory |
For rebar bending tests |
05.6 |
|
12 |
Bending test machine |
GG-2.5 |
Tianjin ZhenHui building Instrument Co., Ltd. |
For the detection of flexible of the product film |
05.12 |
|
13 |
-30 Low temperature box |
DX30-130 |
Beijing lili cryogenic equipment co., LTD |
Pre- frozen of low temperature bending experiment |
05.8. |
|
14 |
Cascade -60 Cascade low temperature cabinet |
-60FDW/200 |
Beijing lili cryogenic equipment co., LTD |
Pre- frozen of freeze-thaw cycle test and low temperature bending experiments |
09、2 |
|
15 |
Electric heated water bath two sets |
DK-98-II |
Tianjin Taisite Instrument Co., Ltd. |
Used for sample adhesion experiment |
05.08 |
|
16 |
Series of impact testing machine |
QJL |
Tianjin Materials experimental train factory |
For impact test, impact strength of film at different height inspection |
05.12 |
|
17 |
Far infrared thermometer（Thermometer） |
RAYMT4V |
Beijing LeiTai Optoelectronic Technology Co. , Ltd. |
To measure the spouts temperature |
05.12 |
|
18 |
Microscope |
XSP-604 |
Phoenix Optical Instrument Group Co., Ltd. |
To observe the porosity of the film |
08.4 |
|
19 |
Microscope |
KSP-02 |
Phoenix Optical Instrument Group Co., Ltd. |
To observe the porosity of the film |
04.4 |
|
20 |
Reading microscope 2 sets |
WYSK-40 |
Phoenix Optical Instrument Group Co., Ltd. |
To observe the porosity of the film |
04.4 |
|
21 |
Reading microscope 2 sets |
10085-1 |
Phoenix Optical Instrument Group Co., Ltd. |
To observe the porosity of the film |
04.4 |
|
22 |
Electric drum wind drying oven 8 sets |
DGG-101-0 |
Shanghai JinPing Instrument Co., Ltd. |
For measuring the Volatile matter of the cathodic disbonding and raw materials and finished products |
07.12 |
|
23 |
Electric drum wind drying oven 4 sets |
DGG-101-2 |
Shanghai Jinping Instrument Co., Ltd. |
For measuring finished cathodic disbonding |
08.9 |
|
24 |
Electric drum wind drying oven 1 sets |
DGG-101-2 |
Tianjin Experimental Instrument Factory |
For measuring finished cathodic disbonding |
08.3 |
|
25 |
DC stabilized power supply 20 groups |
WYK-302B2 |
Easy special Power Systems Ltd. |
To measure electric current and voltage of the cathode stripping |
06. 1 |
|
26 |
Shore hardness tester |
TH210 |
ShangHai LunJie Electrical Instrument Co., Ltd. |
To measure the film hardness |
08.4 |
|
27 |
Each two temperature measuring pen 165℃-250℃ |
/ |
/ |
To measuring the temperature of the sample |
07.10 |
|
28 |
Gel instrument |
/ |
/ |
To measure powder gel time , making it applicable for site process |
03.6 |
|
29 |
Measuring cylinder |
Ex20 |
Tianjin Northern Glass Instrument Factory |
For Weighing solution |
08.9 |
|
30 |
Pipette 5ml/10ml/20ml |
TH51 |
Tianjin Glass Instrument Factory |
Accurately weighing solution |
07.7 |
|
31 |
Table balance 2 sets |
/ |
/ |
For weighing material used in the research and development experiment |
07.5 |
|
32 |
Long-stem funnel |
75 |
ShenBo Instruments, Inc. |
For measuring powder density |
08.4 |
|
33 |
burette |
Basic |
Tianjin Glass Instrument Factory |
For testing of materials titration and calibration solution |
03.6 |
|
34 |
Asphalt softening point tester |
220V.A |
Tianjin YongLiDa Material Testing Machine Co., Ltd. |
For measuring the softening point of the epoxy and curing agent |
03.9 |
|
35 |
Asphalt softening point tester |
/ |
Tianjin Yu Wen Materials Testing Machine Co. , Ltd. |
For measuring the softening point of the epoxy and curing agent |
03.9 |
|
36 |
Volumetric flask |
50/500ml |
Tianjin Glass Instrument Factory |
For measuring the density of the finished product |
03.6 |
|
37 |
Wide-mouth bottle |
2500ml |
Tianjin Glass Instrument Factory |
For the product of resistance to a solution of corrosive experiment |
04.2 |
|
38 |
Fluidized state analyzer |
/ |
/ |
Simulated field fluidized bed |
06.5 |
|
39 |
Glass instrument airflow dryer |
KQ-C |
Gong Wen City ZiHua Instrument Co., Ltd. |
Used for rapid drying of various kinds of glass apparatus |
08.4 |
|
40 |
Sample pressure instrument |
YP-2 |
Shanghai ShanYue Scientific Instruments Co. , Ltd. |
For sample preparation |
03.8 |
|
41 |
Micrometer |
0-25mm |
HangZhou Iinstrument factory |
For measuring the level of liquidity in diameter |
03.8 |
|
42 |
Vernier caliper |
0-200mm |
HangZhou Instrument factory |
For measuring the level of liquidity in diameter |
05.6 |
|
43 |
Multimeter |
DT9280 |
XianBa Electronic Instrument Co., Ltd. |
For measuring the voltage and the current of cathode stripping |
03.9 |
|
44 |
Multimeter |
DT9205 |
XianBa electronic Instrument Co., Ltd. |
For measuring the voltage and the current of cathode stripping |
08.10 |
|
45 |
Paint film scriber |
QFH |
The Tianjin JingKe material testing machine factory |
For measuring adhesion of paint film |
03.9 |
|
46 |
Stopwatch |
JS-306 |
ShenZhen JunSiDa Industrial Co., Ltd. |
For measuring the gel time |
03.6 |
|
47 |
Variable resistance box 40 sets |
ZX21 |
TianShui Changcheng Electrical Instrument Factory |
For cathode stripping |
07.12 |
|
48 |
Slide rheostat 90 sets |
J2354 |
NanTong XinShen Resistor Ltd. |
For cathode stripping |
09.2 |
|
49 |
Standard sieve |
60 mesh |
ZhenXing Sieve with Factory |
For measuring the sieve residue |
03.6 |
|
50 |
Standard sieve |
80 mesh |
ZhenXing Sieve with Factory |
For measuring the sieve residue |
03.6 |
|
51 |
Standard sieve |
400 mesh |
ZhenXing Sieve with Factory |
For measuring pigments and fillers sieve residue |
03.6 |
|
52 |
Standard sieve |
500mesh |
ZhenXing Sieve with Factory |
For measuring pigments and fillers sieve residue |
03.6 |
|
53 |
Dryer |
/ |
Tianjin Glass Instrument Factory |
Place objects easy absorption of moisture |
06.2 |
|
54 |
Universal electronic furnace |
220V-AC |
Tianjin Taisite Instrument Co., Ltd. |
For measuring the gel time |
07.1 |
|
55 |
Rotameter |
LZB-10 |
Yuyao automation instrument factory |
For Measuring powder fluidization state |
07.12 |
|
56 |
Electrically heated distilling water apparatus |
HS.268.5 |
Bright Medical Instrument Factory |
For preparation of distilled water |
09.2 |
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1. Infrared Spectrometer |
2.DSC（Differential Scanning Calorimetry）
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3. Laser Particle Size Distribution Analyzer |
4. Atomic AbsorptionSpectrometry
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5. Electronic Precision Balance
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6. The Cathode Stripping Device |
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7. Water Bath
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8. High Impedance Meter
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9. Bending Machine |
10. Cathode Stripping O ven |
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11. Paint Film Scriber |
12. Microscope |
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13. Impact Tester |
14. UV Curing Lamp |
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15. Gel Instrument |
16. Magnetic Material Analyzer |
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17Wide Mouth Bottle |
18. Standard Sieve |
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19.-30oC FDW/200 Cascade Low Temperature Cabinet |
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21. EDM Leak Detector |
22. Thickness Gauge |
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23.LS Dual-Function Infrared Thermometer |
24. Mechanical Overweight Analytical Balance |
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26. Epoxy Value Analyzer
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27. Softening Point Tester |
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28. Determination of Inorganic A hlorine
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29. Organic Chlorine Analyzer
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19.5 OUTRE finished product quality control
Outre inspects manufactured products strictly in accordance with the requirement of the project standards. Outre has a heavy-duty anti-corrosion testing center, and our center is equipped with a full set of anti-corrosion powder detection laboratory instruments. In order to ensure the product quality of heavy-duty coatings we signed a long-term technical cooperation agreement with Comprehensive Test Center of China Petroleum Pipeline Company, so as to provide reliable quality assurance for the product into the market.
19.5.1 Comprehensive testing of the finished products
In the production process, we test the anti-corrosion performance of the powder and coating quality indicators, including the particle size distribution(GB/T6554), density(GB/T4472), volatiles(GB/T6554), gel time(GB/T6554), curing time(GB/T23257-2009), adhesion(GB/T23257-2009), cathode stripping(GB/T23257-2009), low temperature bending(GB/T23257-2009), thermal characteristics(GB/T23257-2009), freeze-thaw cycle, the magnetic content(GB/T4472), volume resistivity (GB/T23257-2009), similarity and so on. Guarantee the materials through the relevant standards and corresponding performance test required by technical specification of the project before use,. And provide gel time curve and curing time curve for preserving pant products, which can be used as the theoretical basis of the on-site debugging process.
After a period of training and improvement in process control, quality inspectors not only make the necessary testing for the general performance of the powder such as gel time, screening, flexibility, but also supervise the raw material weighing until the packaged sealing of the finished products. We control every aspect strictly to ensure the factory pass rate of 100%.
19.5.1 Finished product quality control table
|
number |
Test items |
Purpose |
Testing frequency |
|
1 |
Similarity≥99.5% |
To ensure the stability of the product |
Each kettle once |
|
2 |
Thermal Characteristics |
To ensure thermal characteristics to meet the standard requirements |
Each kettle once |
|
3 |
Particle size distribution |
1、The monitoring of the production 2、Powder coating particle size distribution is more concentrated, more reasonable distribution , increasing the rate of powder utilization |
Each kettle once |
|
4 |
Density |
To ensure that the content of the resin in the powder composition |
Each kettle once |
|
5 |
Volatile matter |
To ensure no seamless point appears during the product spraying process |
Each batch once |
|
6 |
Gelling time |
provide the reference information for spraying process |
Each kettle once |
|
7 |
Curing time |
Provide reference information for the spraying process , to ensure the film quality |
Each batch once |
|
8 |
Adhesion |
Make the coating has a good adhesion |
Each batch once |
|
Cathode stripping |
The coated specimen has the good cathodic protection |
Each kettle once |
|
|
10 |
Cold bend |
Guarantee spraying specimen without damage during transport |
Each kettle once |
|
11 |
Freeze-thaw cycles |
To ensure that the product is able to adapt the strong temperature changes |
Each batch once |
|
12 |
Magnetic content |
Less magnetic material can reduce the corrosion point |
Each kettle once |
|
13 |
Volume resistivity |
To ensure product insulation class |
Each batch once |
|
14 |
Hardness |
Ensure that the scratch resistance and resistance to collision of anti-corrosion layer in the construction and transport process |
Each batch once |
|
15 |
Wear resistance |
Ensure that the scratch resistance and resistance to collision of anti-corrosion layer in the construction and transport process |
Each batch once |
|
16 |
Powder Appearance |
Ensure powder color uniformity , no lumps |
Each kettle once |
|
17 |
Flow coefficient |
Ensure the smooth progress of spraying |
Each kettle once |
|
18 |
Sieve residue |
Ensure uniform powder，spraying is carried out smoothly |
Each kettle once |
|
19 |
Hiding power |
To ensure that the hiding power of powder products |
Each batch once |
|
The level of liquidity |
to ensure the integrity of the film，no seamless point |
Each batch once |
|
|
21 |
Heat resistance |
To ensure the storage stability of the powder |
Each batch once |
|
22 |
Glass transition temperature |
To ensure the storage stability of the powder |
Each kettle once |
|
23 |
Gelling curve |
Provide data information for spraying |
Each batch once |
|
24 |
Curing curves |
Provide data information for spraying |
Each batch once |
|
Once powder utilization |
To ensure powder utilization |
Each batch once |
|
|
26 |
Impact resistance |
Ensure anti-corrosion layer in the process of construction and transportation crashworthiness |
Each kettle once |
|
27 |
Porosity |
To ensure water resistance and solvent resistance of the film |
Each batch once |
|
28 |
Film appearance |
To ensure the integrity of the film after the spraying |
Each kettle once |
|
29 |
Curing percentage |
Ensure the degree of cure of the film after spraying |
Each batch once |
|
30 |
Electrical strength |
To ensure the film's insulation |
Each batch once |
|
31 |
Chemical resistance |
To ensure the chemical resistance of the anti-corrosion layer |
Each batch once |
|
32 |
Salt spray test |
To ensure the corrosion resistance of the corrosion protective layer |
Each batch once |
19.5.2 Detection introduction to detailed indicators
Currently, Outre has advanced testing instruments such as differential scanning calorimetry , infrared spectroscopy , laser particle size distribution analyzer , atomic absorption spectrometer , impedance meter, magnetic material analyzer and so on，Providing a reliable guarantee for the control of product quality .
1. Finished products similarity detection ：Infrared spectrometer can be used for qualitative and quantitative analysis of materials . Each kettle products sampling are analysed by the infrared spectroscopy , and compare infrared similarity of the products of different kettle, so as to we can control the product quality stability strictly.
2. Thermal characteristics indicator detection of ΔH 、Tg2、 △Tg2 and so on
Outre has imported advanced the DSC（Differential scanning calorimetry） detection instrument , and a full range of thermal characteristics analysis is carried on powder products : as heat release ΔH can ensure that the resin content in the powder , Tg1 can provide a reference for the storage stability of the powder , Tg2 can monitor the heat resistance of the coating after made into the film , but also we can measure Tg3 and Tg4 , so as to get ΔTg， measuring cured percentage .
3. Product particle size distribution tests : Outre has an advanced laser particle size distribution analyzer which can effectively monitor the production process of the powder , the product of good particle size distribution plays an extremely important role in the latter part of the powder utilization.
4. Pigments and fillers purity test: Outre has imported an atomic absorption spectrometer that can test the content of metal elements in the pigments and fillers , which can analyze the purity of the pigments and fillers.
5. -60oCFDW/200 Cascade Low Temperature Cabinet: measure hot and cold cycle
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6. Cathodic disbanding device |
7. Water bath: For boiled adhesion test |
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8. The Low Temperature Box: For bending test |
9. Bending Instrument: For bending test |
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10. Oven and Voltage-Stabilized Source: For Cathodic disbanding test |
11.Gel Instrument : For gel time test |